HPLC Method for Analysis of Poly(propylene glycol) bis(2-aminopropyl ether) on Primesep 200 Column by SIELC Technologies

HPLC-Applikation • Datum: 2022/11/07
HPLC Method for Analysis of Poly(propylene glycol) bis(2-aminopropyl ether) on Primesep 200 Column by SIELC Technologies Chromatogramm

Poly(propylene glycol) bis(2-aminopropyl ether) is a hydrophobic polymer with the chemical formula CH3CH(NH 2 )CH 2 [OCH2CH(CH 3 )] n NH 2 . It is primarily used in preparation of epoxy resins or as a proton acceptor in nanocomposites for CO2 capture.

Poly(propylene glycol) bis(2-aminopropyl ether) can be retained and analyzed using the Primesep 200 stationary phase column. The analysis utilizes an isocratic method with a simple mobile phase consisting of water and acetonitrile (MeCN) with a [buffer] buffer. Detection is performed using UV.

Methodenparameter

ColumnPrimesep 200, 3.2 x 100 mm, 5 µm, 100 Å, dual ended
Mobile PhaseGradient MeCN10 – 60%, 20 min
BufferTFA – 0.2%
Flow Rate0.5 mL/min
DetectionELSDT50C