HPLC Determination of Resorcinol Diglycidyl Ether on Newcrom R1
https://sielc.com/hplc-determination-of-resorcinol-diglycidyl-ether-on-newcrom-r1Chromatogram
Description
· High Performance Liquid Chromatography (HPLC) Method for Analysis of Diglycidyl resorcinol ether .
Diglycidyl Resorcinol Ether , also called Resorcinol diglycidyl ether (RDGE), is a glycidyl ether with the C 12 H 14 O 4 . It is commercially available to reduce viscosity of epoxy resins. It is also highly toxic, potentially leading to irritation of skin, eyes, respiratory system, and skin. It is a known carcinogen with no safe levels of exposure.
Diglycidyl resorcinol ether can be retained and analyzed using the Newcrom R1 stationary phase column. The analysis utilizes an isocratic method with a simple mobile phase consisting of water and acetonitrile (MeCN) without a buffer. Detection is performed using UV.
Method Parameters
| Mobile Phase | MeCN/H2O – 30/70% |
|---|---|
| Buffer | No |
| Flow Rate | 1.0 ml/min |
| Detection | UV 220 nm, MS-compatible mobile phase |
| Class of Compounds | Hydrophobic, Neutral |
| Analyzing Compounds | Diglycidyl resorcinol ether |
HPLC Column Used
Newcrom R1, 3.2 x 50 mm, 3 µm, 100 A, dual ended